DGR

Make : LECO Corporation, USA

Model : FP 528

Specification :

Readability: 0.001%, Calibration: Standard Sample; Linear, Analysis Time: 3 minutes, Sample Size: Up to 250 mg, Detection Method: Thermal Conductivity, Furnace Range: Up to 975o Celsius

The sample were placed into a hot furnace and flushed with pure oxygen for very rapid combustion.
Where by nitrogen containing material is converted to molecular nitrogen and the by-products of combustion (CO2, H2O, NOx, and N2) pass through the furnace filter and thermoelectric cooler for subsequent collection in a ballast apparatus.
These collected gases in the ballast are mixed, and a small aliquot dose is then used for further conversion of the gases.
The remaining aliquot that has been reduced is measured by the thermal conductivity cell for Nitrogen.

MAIN FEATURES OF THE INSTRUMENT

FEATURES
Instrument Range	Helium Model (3 cc Aliquot Loop): 0.04 mg to 250 mg absolute Nitrogen ;Argon Model (10 cc Aliquot Loop): 0.1 mg to 100 mg absolute Nitrogen
Precision	Helium Model (3 cc Aliquot Loop): 0.02 mg or 0.5% RSD, whichever is greater ;Argon Model (10 cc Aliquot Loop): 0.05 mg or 1.0% RSD, whichever is greater
Readability	0.001%
Calibration	Standard Sample; Linear
Analysis Time	3 minutes
Sample Size	Up to 250 mg
Detection Method	Thermal Conductivity
Chemical Reagents	Anhydrous Magnesium Perchlorate, Calcium Oxide, Sodium Hydroxide on an inert base, Copper Sticks, N Catalyst Reagent, Copper Turnings, Alumina Pellets, Magnesium Oxide
Gas Required	Carrier Gas: 99.99% Helium or Argon, 40 psi (2.8 bar), ±10% , Combustion Gas: 99.99% Oxygen, 40 psi (2.8 bar), ±10% ;Pneumatic Gas: Compressed Air, 40 psi (2.8 bar), ±10%.
Gas Flow Rates	Carrier Gas: Analysis 200 mL/min (measure), 30 mL/min (reference), Conservation: 30 mL/min (measure), 30 mL/min (reference), ;Combustion Gas: 1.3 to 6 L/min (user programmable oxygen profile)
Furnace Range	Up to 975° Celsius
Electrical Power Requirements	230 V~ (±10%; at max load), 50/60 Hz, single phase, 10 A, 7,900 BTU/hr

• Used for the estimation of total nitrogen present in the sample.
• Nitrogen/Protein analyser is an alternative method of Kjeldahl.

1. https://www.leco.com/products/analytical-sciences/nitrogen-protein-analyzer/fp528
2. http://leco-korea.com/wi_files/item_pdf/25_70.pdf

1. Sample should be preferably submitted in pulverized form.
2. Sample requirement: 2-5 g

Contact :+91-9725018784 Email Id : mahesh.mahatma@icar.gov.in

Nitrogen Analyser charges (Rs)includes GST

	Industry	University	National Lab/R&D's
Standardization	1000	400	500	Per Parameter
Sample estimation	800	200	300	Per Sample
Sample preparation	200	50	100	Per Sample